13889-98-0, 1-Acetylpiperazine is a piperazines compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
General procedure P. l-[4-(4-Nitro-phenyl)-piperazin-l-yl]-ethanoneA focus microwave vessel was charged with 4-fluoronitrobenzene (leqv, 1.41 g, 10 mmol), acetylpiperazine (leqv, 1.28 g, 10 mmol), DIPEA (leqv, 1.7 ml, 10 mmol) and propan-2-ol (2 ml). The reaction mixture was irradiated (100W) at 9O0C for 25 mins. A yellow precipitate formed on cooling, which was collected by filtration, washed with propan-2-ol (20 ml) and dried under vacuum to give the product (1.401 g, 56%, 5.6 mmol) as a yellow solid. LC/MS: 100% MH+, m/z 250, Rt = 1.23 mins.
13889-98-0, 13889-98-0 1-Acetylpiperazine 83795, apiperazines compound, is more and more widely used in various fields.
Reference£º
Patent; EVOTEC AG; WO2008/122787; (2008); A1;,
Piperazine – Wikipedia
Piperazines – an overview | ScienceDirect Topics