13889-98-0, 1-Acetylpiperazine is a piperazines compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
Step 2: Preparation of 1-(4-(3-methoxy-4-nitrophenyl)piperazin-1-yl)ethanone The compound obtained in Step 1 above (300 mg), N-acetylpiperazine (300 mg), and potassium carbonate (500 mg) were dissolved in dimethylformamide (3 mL) and reacted at 80C overnight. The dimethylformamide of the reaction mixture was removed under reduced pressure, and added with water to form a solid. The solid was filtered to obtain a target compound as a yellow solid. 1H-NMR(300 MHz, CDCl3) delta 8.00(d, J = 9.1 Hz, 1H), 6.42(d, J = 9.1 Hz, 1H), 6.32(s, 1H), 3.96(s, 3H), 3.80-3.79(m, 2H), 3.67-3.65(m, 2H), 3.47-3.40(m, 4H), 2.15(s, 3H); Mass (M+H+) calcd for C13H17N3O4 279.12, found 279.20, 13889-98-0
13889-98-0 1-Acetylpiperazine 83795, apiperazines compound, is more and more widely used in various fields.
Reference£º
Patent; Korea Research Institute of Chemical Technology; LEE, Kwangho; KIM, Hyoung Rae; PARK, Chi Hoon; LEE, Chong Ock; LEE, Jong Kook; JUNG, Hee Jung; CHO, Sung Yun; CHAE, Chong Hak; CHOI, Sang Un; HA, Jae Du; EP2883875; (2015); A1;,
Piperazine – Wikipedia
Piperazines – an overview | ScienceDirect Topics