76003-29-7, 1-Boc-3-Oxopiperazine is a piperazines compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
To a solution [OF TERT-BUTYL 3-OXOPIPERAZINE-1-CARBOXYLATE] (0.500 mg, 2. [50] mmol) in 10 mL of DMF at [0 C] was added NaH as a 60% dispersion in mineral oil (2.62 mmol), and the reaction was stirred for 45 minutes. [4-BROMO-1-BUTENE] was added (0.280 mL, 2.75 mmol) dropwise as a solution in 1 mL of THF. The solution was stirred overnight, allowing it to warm to room temperature. The reaction was partitioned between EtOAc and saturated [NAHC03] solution. The organic phase was washed with brine, dried [(NA2S04),] filtered, and concentrated in vacuo to give the titled compound. Proton NMR for the product was consistent with the titled compound. ESI+MS : 255.1 [[M+H]] [+.], 76003-29-7
As the paragraph descriping shows that 76003-29-7 is playing an increasingly important role.
Reference£º
Patent; MERCK & CO., INC.; WO2004/14851; (2004); A2;,
Piperazine – Wikipedia
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