50606-32-1, Butyl piperazine-1-carboxylate is a piperazines compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
50606-32-1, 56.2. 4-[2-Benzyloxycarbonylamino-2-(dimethoxy-phosphoryl)-acetyl]-piperazine-l- carboxylic acid butyl ester: To a solution of intermediate 56.1 (1.5 g) in DCM (5 mL) was added DIPEA (3.4 mL) and HATU (2.2 g). After stirring at RT for 10 min, intermediate 2.2 (1.1 g) was added. The reaction mixture was stirred overnight at RT and H2O was added. The phases were separated, the org. phase was washed with sat NaCl solution, dried (MgStheta4) and evaporated off. The crude was purified by CC (Hept/EA 2/8) to afford the desired compound (1.1 g). LC-MS (A): tR = 0.95 min; [M+H]+: 486.01.
The synthetic route of 50606-32-1 has been constantly updated, and we look forward to future research findings.
Reference£º
Patent; ACTELION PHARMACEUTICALS LTD; WO2009/69100; (2009); A1;,
Piperazine – Wikipedia
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